| 1-羟基芘的制备及其质谱光谱解析 |
| 摘要点击 1262 全文点击 1070 投稿时间：1991-12-05 |
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| 中文关键词 1-羟基芘 芘 质谱 光谱 |
| 英文关键词 1-hydroxypyrene pyrene |
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| 中文摘要 |
| 报告了由芘制备1-羟基芘的方法,对所得产品进行了元素含量、质谱、核磁共振、紫外光谱、红外光谱和荧光光谱的分析。确定其组成为C6H10O5,羟基在C1位上;解析了质谱图中主要裂解产物的结构;给出特征光谱图,克分子消光(λ345nm)为3822.6。产品为较好的色谱纯品。 |
| 英文摘要 |
| A procedure for the preparation of 1-hydroxypyrene from pyrene was described. Its mass spectrum, nuclear magnetic resonance, infrared, ultraviolet and fluorescence spectra were determined. The results show that the compound thus prepared is a very pure product. |
